Synthesis of boron carbide from its elements up to 13 GPa
نویسندگان
چکیده
The formation of boron carbide under high pressures and from elemental reactants has been studied optimum parameters have determined by varying the (P, T, reactants) conditions. To this end, stoichiometric mixtures commercial beta rhombohedral amorphous glassy carbon subjected to temperatures ranging 1473 K 2473 at 2 GPa, 5 GPa 13 GPa. Similar syntheses repeated for graphite, concentration is shown be affected pressure which it synthesised elements, we propose as a means control content. temperature choice reactants. effect cycling on also studied. alpha an intermediate phase seen before carbide.
منابع مشابه
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ژورنال
عنوان ژورنال: Journal of Physics and Chemistry of Solids
سال: 2021
ISSN: ['0369-8726', '0022-3697', '1879-2553']
DOI: https://doi.org/10.1016/j.jpcs.2021.110253